Colonnes Ohio Valley


 

Volatils

Nitroaromatiques

Aromatiques

Mélange de TCLP

Mélange de phénols

Essence

Mélange hydrocarbures (Diesel)

EPA Méthode 606 Phthalates

EPA Méthode 611 hydrocarbures chlorés EPA Méthode 612 hydrocarbures chlorés

 

Volatils
30 Meters x 0.53 mm 
OV-624, 3.0 µm Film
Catalog N° 630-5307
Direct injection 1µl (split)
Oven : 5°C (Hold 5 min.)
--> 200°C at 10°C/min
1µl Temp 225°C
Detector Temp 250°
GC/MS Detector

1. Chloroform
2. Bromodichloromethane
3. Dibromochloromethane
4. 1, 2-Dibromoethane
5. Bromoform
6. 1, 2-Dibromo
3 Chloropropane
Nitroaromatiques
15 Meters x 0.53 mm 
OV-5, 1.5 µm Film, 
Catalog N° 515-5310
0.5µl split injection
Oven 100°C 
--> 300°C at 15°C/minute 
1µl Temp 250°C
Detector Temp 30°
Detector F. I. D.

1. Nitrobenzene
2. Isophorone
3. 2, 6-Dinitrotoluene
4. 2, 4-Dinitrotoluene

 

Aromatiques
30 Meters x 0.32 mm OV-1, 0.5 µm Film
Catalog N° 130-3203
0.5µl split injection (50:1)
Oven 60°C --> 250°C at 4°C/minutes
1µl Temp 250°C
Detector Temp 250°
Detector : F. I. D.

1. Methylene chloride
2. Propylene glycol
3. Eucalyptol
4. Menthol
5. Methyl salicylate

Mélange de TCLP 
30 Meters x 0.25 mm OV-5, 
0.5 µm Film
Catalog N° 530-2503
1.0 µl split injection(50:1 split)
Concentration 1000µl/ml
Oven : 35°C (hold 8 min)
--> 250°C at 5°C/min
1µl Temp 200°C
Detector Temp 285°
Carrier Gas : Helium
Detector : GC/MS

1.Vinyl Chloride
2.1, 1-Dichloroethane
3.2-Butanone
4.Chloroform
5.1, 2-Dichloroethane
6.Benzene/cc14
7.Fluorobenzene (IS#1)
8.Trichloroethane
9.2-Bromo-1-chloropropane (IS#2)
10.Tetrachloroethene
11.Chlorobenzene
12.1, 4-dichlorobenzene

 

Mélange de phénols 

30 Meters x 0.25 mm OV-5, 0.25 µm Film
Catalog N° 530-2502
1.0µl split injection
8-10 µg/µl per component
Oven : 50°C (Hold 3 minutes)
--> 250°C at 8°/minutes
1µl Temp 250°C
Detector Temp 250°C
split injection (50:1)

Essence

30 Meters x 0.32 mm OV-5, 1.0 µm Film Catalog N° 530-3204
40°C (Hold 6 minutes) --> 250°C at 5°/minutes (at 250°C, hold 70 minutes)
Injection Temperature 250°C, Detector Temperature 275°C, Dectecto F. I. D.

1. Methane
2. Ethane
3. Propane
4. Butane
5. Pentane
6. Hexane
7. Benzene
8. Heptane
9. Octane
10. Nonane
11. C10
12. C11
13. C12
14. C13
15. C14
1. Phenol
2. 2-Chlorophenol
3. 2-Nitrophenol
4. 2, 4-Dimethylphenol
5. 2, 4-Dichlorophenol
6. 4-Chloro-3-methylphenol
7. 2, 4, 6-Trichlorophenol
8. 2, 4-Dinitrophenol
9. 4-Nitrophenol
10. 2-Methyl 4, 6-Dinitrophenol
11. Pentachlorophenol

 

Mélange hydrocarbures (Diesel)

30 Meters x 0.25 mm OV-5, 1.0 µm Film, Catalog N° 530-2504
100°C --> 340°C at 15°/minutes (Hold 10 minutes)
Injection Temperature 250°C,Detection Temperature 340°C

Detector F. I.D.

EPA Méthode 606 Phthalates

30 Meters x 0.25 mm OV-5, 0.50 µm Film
Catalog N° 530-2503
200°C --> 310°C at 13°C/minute (Hold 15 minutes)
Injection Temperature 300°C
Detection Temperature 320°C, Detector F. I. D.

1. Methanol
2. Dimethyl Phthalate
3. Di-N-Butyl Phthalate

4. Butyl Benzyl Phthalate
5. Bis(2-Ethylhexyl) Phthalate
6. Di-N-Octyl Phthalate

1. Decane
2. Dodecane
3. Tetradecane
4. Hexadecane
5. Octadecane
6. Eicosane
7. Docosane
8. Tetracosane
9. Hexacosane
10. Octacosane

 

EPA Méthode 611 hydrocarbures chlorés

30 Meters x 0.25 mm OV-5, 0.50 µm Film Catalog N° 530-2503
Temperature Program 100°C --> 250°C at 15°C/minute
Injection Temperature 250°C
Detection Temperature 300°C, Detector F. I. D.

1. Bis (2-Chloroisopropyl) Ether
2. Bis (2-Chloroisopropyl) Ether
3. Bis (2-Chloroethoxy) Methane
4. 4-Chlorophenyl Phenyl Ether
5. 4-Bromophenyl Phenyl Ether

EPA Méthode 612 hydrocarbures chlorés

30 Meters x 0.25 mm OV-5, 0.50 µm Film 
Catalog N° 530-2503
Temperature Program 40°C --> 250°C at 10°C/minute
Injection Temperature 300°C
Detection Temperature 350°C, Detector F. I. D.

1. 1, 3-Dichlorobenzene
2. 1, 4-Dichlorobenzene
3. 1, 2-Dichlorobenzene
4. Hexachloroethane
5. 1, 2, 4-Trichlorobenzene
6. Hexachlorobutadiene
7. Hexachlorocyclopentadiene
8. 2-Chloronapthalene
9. Hexachlorobenzene

 

Colonnes:

213,avenue Kennedy-BP 1140

03103 Montluçon Cedex-France

Tel 33 (0) 4.70.03.73.09 

Fax 33 (0) 4.70.03.82.60 

interchrom@interchim.com

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